Preparation of p-phenyl sulfonate esters of acyl glycolic acids

Organic compounds -- part of the class 532-570 series – Organic compounds – Fatty compounds having an acid moiety which contains the...

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562590, 554 91, 560142, C07C 6729

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active

051244756

ABSTRACT:
The invention encompasses methods for preparing in high purity and in high yield p-phenyl sulfonic acid acyl glycolates of the formula ##STR1## where R represents branched or straight chain alkyl having 6-12 carbon atoms by treating a phenyl ester or phenyl acyl glycolate of the formula ##STR2## where R represents branched or straight chain alkyl having 6-12 carbon atoms with a sulfonating agent to form intermediate sulfonation; transmuting the intermediate sulfonation products; and quenching the transmuted intermediate sulfonation products with a quenching reagent reactive with sulfur trioxide.

REFERENCES:
patent: 4588333 (1986-05-01), Berry
patent: 4692279 (1987-09-01), Nussbaum
patent: 4705649 (1987-11-01), Balzer et al.
patent: 4735740 (1988-05-01), Zielske
patent: 4959187 (1990-09-01), Fong et al.

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