Preparation of o-(1-methoxy-2-chloro)-ethoxyphenyl N-methylcarba

Details Preparation of o-(1-methoxy-2-chloro)-ethoxyphenyl N-methylcarba Preparation of o-(1-methoxy-2-chloro)-ethoxyphenyl N-methylcarba

1987-09-25

1988-11-29

Shaver, Paul F.

Organic compounds -- part of the class 532-570 series

Organic compounds

Carboxylic acid esters

C07C17504

Patent

active

047883243

ABSTRACT:
O-(1-Methoxy-2-chloro)ethoxyphenyl N-methylcarbamate is prepared by reacting pyrocatechol carbonate with methylamine and then reacting the resulting pyrocatechol monomethylcarbamate with 1,2-dichloroethyl methyl ether in the presence of a secondary amine.

REFERENCES:
patent: 3962316 (1976-06-01), Kiehs et al.
patent: 4537986 (1985-08-01), Reissenweber et al.
Loeffler et al., Derwent Abstract No. 35128A (abstract of DE 2650828).
Kirk-Othmer, Encyclopedia of Chemical Technology, 2nd ed., vol. 2, 1963, pp. 103-105, 110-112 and 127-133.
Noller, Chemistry of Organic Compounds, 2nd ed., 1957, pp. 233-237 QD 253 N65.
Liebigs Ann. Chem. 300 (1898) p. 135.
Liebigs Ann. Chem. 362 (1949) p. 205.
J. prakt. Chem. 313 (1971) p. 626.

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