Preparation of microcrystalline triacetylcellulose

Organic compounds -- part of the class 532-570 series – Organic compounds – Carbohydrates or derivatives

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210635, 2105021, 502439, 536 69, 536 73, 536 74, 536 76, C08B 306

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046970070

ABSTRACT:
The preparation of microcrystalline triacetylcellulose by acid-catalyzed acetylation of microcrystalline cellulose, perfluoroalkanesulfonic acids with 1 to 8 carbon atoms are used as the catalyst, resulting in a non-hazardous process and high yields of exceptionally high purity product, the latter being particularly suitable for chromatographic purposes, in particular for the chromatographic resolution of racemates.

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patent: 3598245 (1971-08-01), Determann
patent: 3632843 (1972-01-01), Allen et al.
patent: 3843702 (1974-10-01), Montigny et al.
patent: 4521308 (1985-06-01), Brimhall, Jr.
patent: 4547474 (1985-10-01), Olah
The Condensed Chemical Dictionary-Eight edition by Hawley, Van Nostrand Reinhold Co. of New York, pp. 85 and 397, 1971.

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