Preparation of methoxy phenyl phosphides

Details Preparation of methoxy phenyl phosphides Preparation of methoxy phenyl phosphides

1988-03-30

1989-12-26

Doll, John

Organic compounds -- part of the class 532-570 series

Organic compounds

Phosphorus containing

C07F 928

Patent

active

048899569

ABSTRACT:
Benzyl- or allyl- di(polar-substituted-phenyl)phosphines are converted in good yield to the corresponding alkali metal di(polar-substituted-phenyl)phosphide by reaction with alkali metal in liquid ammonia.

REFERENCES:
patent: 2437795 (1948-03-01), Walling
patent: 4393240 (1983-07-01), Stille
patent: 4687874 (1987-08-01), Oswald et al.
Inorganic Syntheses, vol. 6, 1975, pp. 155-161, V. D. Blanco et al: Tertiary Phosphines.
Chemistry and Industry, 10/24/70, p. 1378, S. O. Grim et al: A Novel Syntheses of Unsymmetrical Ditertiary Phosphines.
Brown et al., Tetrahedron Letters, vol. 21, pp. 581-584, (1980).

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