Preparation of metal powders

Specialized metallurgical processes – compositions for use therei – Compositions – Loose particulate mixture containing metal particles

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75 05A, 75 89, 75 97A, 75117, 75118R, 75121, 75252, 148 13, 148 131, 148 132, 148 206, 1481261, 419 2, 419 23, 419 32, 419 34, 419 62, 420469, 420590, B22F 100

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046157360

ABSTRACT:
A process is disclosed for the preparation of metallic products from metal salts admixed with solvent wherein at least one of the metal salt and the solvent is easily reducible. The admixture is heated under hypercritical conditions of temperature and pressure to produce metallic products and a hypercritical fluid. The hypercritical fluid is subsequently removed from the reaction zone and the metallic product is collected. The metallic product includes pure metals selected from the group of silver, gold, platinum, palladium, ruthenium, rhodium, mercury, arsenic, rhenium, tellurium, iridium, osmium, and copper, and alloys and mixtures thereof. The metallic product ordinarily exists as finely divided powders which may be highly porous.

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Danforth et al., "Synthesis of Ceramic Powders by Laser Driven Reactions", Industrial Liason Program No. 10-17-82, ILP Publications Office, MIT, Cambridge, MA.
S. J. Teichner et al., "Inorganic Oxide Aerogels", Advanced in Colloid and Interface Science, vol. 5, 1976, pp. 245-273.

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