Preparation of lower trialkyltin hydride from trialkyltin chlori

Details Preparation of lower trialkyltin hydride from trialkyltin chlori Preparation of lower trialkyltin hydride from trialkyltin chlori

1980-04-11

1981-08-04

Sneed, Helen M. S.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07F 722

Patent

active

042821665

ABSTRACT:
A simple, direct, and safe process for preparing an organic solvent solution of a lower trialkyltin hydride of high purity and in high yield by reacting a lower trialkyltin chloride with an alkali metal bis(2-alkoxyethoxy)aluminum dihydride in a hydrocarbon solvent boiling in the 50.degree. to 200.degree. C. range.

REFERENCES:
patent: 3281443 (1966-10-01), Hunt
patent: 3347891 (1967-10-01), Neumanu et al.
patent: 3379747 (1968-04-01), Itoi
patent: 3439010 (1959-04-01), Okawara et al.
patent: 3507895 (1970-04-01), Casensky et al.
patent: 3758620 (1973-09-01), Vit
Chemical Abstracts, 55 27809h, (1967).
Finholt et al., JACS 69 2692-2696, (1947).
Vit et al., Eastman Organic Chemical Bulletin, vol. 46, No. 1, p. 5, (1974).
Fish et al., JACS 89 5861, (1967).

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