Preparation of J-acid urea

Organic compounds -- part of the class 532-570 series – Organic compounds – Sulfonic acids or salts thereof

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C07B27300

Patent

active

051440644

ABSTRACT:
J-Acid urea of the formula ##STR1## is prepared by reacting 7-amino-4-hydroxynaphthalene-2-sulfonic acid (J-acid) with urea at from 100.degree. to 140.degree. C. under a pressure ranging from atmospheric pressure to 10 bar in an inert solvent to a partial extent, precipitating unconverted J-acid in an acidic medium and separating it off, and, if desired, isolating J-acid urea from the resulting neutralized solution by salting out.

REFERENCES:
patent: 675631 (1901-06-01), Israel et al.
patent: 4599203 (1986-07-01), Conrow et al.

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