Preparation of iron or iron oxide nanoparticles

Chemistry of inorganic compounds – Oxygen or compound thereof – Metal containing

Reexamination Certificate

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

C423S138000

Reexamination Certificate

active

07985398

ABSTRACT:
The present teachings are directed towards a thermolysis method of producing iron-containing nanoparticles by providing an iron-containing component, a colloid stabilizing component, and an amount of water. The iron-containing component, the colloid stabilizing component, and the amount of water form a mixture, which is then heated to a temperature sufficient to form iron-containing nanoparticles, which are then isolated from the mixture. Another method is also provided which involves a repetitive shell growth method of producing iron-containing nanoparticles by providing a first amount of an iron-containing component and a colloid stabilizing component; the iron-containing component and the colloid stabilizing component are then mixed and heated to a temperature sufficient to form iron-containing nanoparticles. The mixture is allowed to cool to room temperature, and an additional amount of iron-containing component is added to the mixture, which is then reheated to reaction temperature, and the process is repeated until the isolated iron-containing nanoparticles obtain the desired size.

REFERENCES:
patent: 5698483 (1997-12-01), Ong et al.
patent: 7410625 (2008-08-01), Sun
patent: 2005/0039382 (2005-02-01), Blanchard et al.
patent: 0 628 612 (1994-12-01), None
patent: 1 249 558 (1971-10-01), None
Shpaisman, N. and Margel, S., “Synthesis and Characterization of Air-Stable Iron Nanocrystalline Particles Based on a Single-Step Swelling Process of Uniform Polystyrene Template Microspheres”, Chem. Mater., vol. 18, pp. 396-402 (2006), American Chemical Society.
Kanzaki, S.; Inada, T.; Matsumura, T.; Sonoyama, N.; Yamada, A.; Takano, M. and Kanno, R., Nano-sized γ -Fe203 as lithium battery cathode, J. Power Sources, vol. 146, pp. 323-326 (2005), Elsevier B.V.
Park, S.; Kim, S.; Lee, S.; Khim, Z.G.; Char, K. and Hyeon, T., “Synthesis and Magnetic Studies of Uniform Iron Nanorods and Nanospheres”, J. Am. Chem. Soc., vol. 122, pp. 8581-8582 (2000), American Chemical Society.
Suslick, K.S.; Fang, M. and Hyeon, T., “Sonochemical Synthesis of Iron Colloids”, J. Am. Chem . Soc., vol. 118, pp. 11960-11961 (1996), American Chemical Society.
Carpenter, E.E.; Calvin, S.; Stroud, R.M. and Harris, V.G., “Passivated Iron as Core-Shell Nanoparticles”, Chem. Mater., vol. 15, pp. 3245-3246, (2003), American Chemical Society.
Burke, N.A.D; Stover, H.D.H. and Dawson, F.P., “Magnetic Nanocomposites: Preparation and Characterization of Polymer-Coated Iron Nanoparticles”, Chem. Mater., vol. 14, pp. 4752-4761 (2000), American Chemical Society.
Ponder, S.M.; Darab, J.G.; Bucher, J.; Caulder, D.; Rao, L.; Shuh, D.K. and Mallouk, T.E., “Surface Chemistry and Electrochemistry of Supported Zerovalent Iron Nanoparticles in the Remediation of Aqueous Metal Contaminants”, Chem. Mater., vol. 13, pp. 479-486 (2001), American Chemical Society.
Lee, J.; Im, S.; Lee, C.; Yu, J.; Choa, Y. and Oh, S., “Hollow nanoparticles of β-iron oxide synthesized by chemical vapor condensation”, J. Nanoparticle Research, vol. 6, pp. 627-631 (2004), Springer.
Ngo, A.T.; Richardi, J. and Pileni, M.P., “Mesoscopic Solid Structures of 11-nm Maghemite, γ-Fe203, Nanocrystals: Experiment and Theory”, Langmuir, vol. 21, pp. 10234-10239 (2005), American Chemical Society.
Huber, D.L., “Synthesis, Properties, and Applications of Iron Nanoparticles”, small, vol. 1, No. 5, pp. 482-501 (2005), Wiley-VCH Verlag GmbH & Co.
S. Sun and H. Zeng, “Size-Controlled Synthesis of Magnetite Nanoparticles,” J.Am.Chem.Soc. Communications, vol. 124, 2002, pp. 8204-8205.
J. Hong et al. “Surface Modification of Hydrophobic Iron Oxide Nanoparticles for Clinical Application,” IEEE Transactions on Magnetics, vol. 41, No. 10, Oct. 1, 2005, pp. 4137-4139.
K. Woo et al., “Easy Synthesis and Magnetic Properties of Iron Oxide Nanoparticles,” Chem. Mater, vol. 16,2004, pp. 2814-2818.
D. Huber et al., “Synthesis of highly magnetic iron nanoparticles suitable for field structuring using a β-diketone surfactant,” Journal of Magnetism and Magnetic Materials, vol. 278, 2004, pp. 311-316.
T. Hyeon et al., “Synthesis of Highly Crystalline and Monodisperse Maghemite Nanocrystallites without a Size-Selection Process,” J. Am. Chem. Soc., vol. 123, 2001, pp. 12798-12801.
D. Huber, “Synthesis, Properties, and Applications of Iron Nanoparticles,” Small-Nano-Micro, Wiley VCH, Weinheim, DE, vol. 1, No. 5, May 1, 2005, pp. 482-501.
M. Hamoudeh et al., “Elaboration of PLLA-based superparamagnetic nanoparticles: Characterization, magnetic behaviour study and in vitro relaxivity evaluation,” International Journal of Pharmaceutics, Amsterdam, vol. 338, No. 1-2, May 23, 2007, pp. 248-257.
International Search Report for PCT/US2007/087045 mailed Jun. 12, 2008.

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Preparation of iron or iron oxide nanoparticles does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Preparation of iron or iron oxide nanoparticles, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Preparation of iron or iron oxide nanoparticles will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-2731345

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.