Preparation of high purity 1,4-butanediol

Details Preparation of high purity 1,4-butanediol Preparation of high purity 1,4-butanediol

1980-07-31

1981-10-13

Trousof, Natalie

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

C07C 2978

Patent

active

042949980

ABSTRACT:
A process for the purification of crude 1,4-butanediol by crystallizing said crude in a solution comprising tetrahydrofuran at a temperature of from 10.degree. to -10.degree. C. and a pressure of from 16-26 mm of mercury to form a slurry of crystallized 1,4-butanediol in a liquid, and then separating the crystallized 1,4-butanediol from the liquid.

REFERENCES:
patent: 2686817 (1954-08-01), Copes et al.
patent: 3467679 (1969-09-01), Rogers
patent: 3852164 (1974-12-01), Chow et al.
patent: 4081257 (1978-03-01), Lassmann et al.
Kirk-Othmer "Encyclopedia of Chemical Technology" Interscience, Publ. 2nd Ed., vol. 10, pp. 249; 668 (1967).
Weissberger, Arnold, Ed. "Techniques of Organic Chemistry" vol. III, Part I, "Separation and Purification", Interscience, Publ. (1956) pp. 396-397, 528-529, 542-543, 548-549 & 555-558.
CRC Handbook of Chemistry and Physics, 60th Edition (1979-1980) pp. C-220 and C-312.

Affiliated with

Also associated with

Rating

Preparation of high purity 1,4-butanediol does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Preparation of high purity 1,4-butanediol, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Preparation of high purity 1,4-butanediol will most certainly appreciate the feedback.

Rate now

Comments { 0 }

Profile ID: LFUS-PAI-O-932315