Preparation of hexaalkyldisilthiane

Details Preparation of hexaalkyldisilthiane Preparation of hexaalkyldisilthiane

1989-03-30

1990-07-24

Shaver, Paul F.

Organic compounds -- part of the class 532-570 series

Organic compounds

Silicon containing

C07F 708

Patent

active

049436473

ABSTRACT:
Hexaalkyldisilthiane compounds (e.g., hexamethyldisilthiane) are synthesized by reaction of lithium disulfide and a halotrialkylsilane (e.g., chlorotrimethylsilane) in a non-oxygenated solvent (e.g., acetonitrile).

REFERENCES:
patent: 3344161 (1967-09-01), Moedritzer et al.
Moehs et al., "J. Org., Nucl. Chem.", 43, No. 2, 1981, pp. 235-237.
Olah et al., "J. Org. Chem.", 44, No. 24, pp. 4272-4275 (1979).
Chanpetier et al., "Compt. Rend.", 234, pp. 1985-1986 (1952).
Detty et al., "J. Org. Chem.", 47, 1982, pp. 1354-1356.

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