Preparation of hexaalkylcyclotrisilthiane

Details Preparation of hexaalkylcyclotrisilthiane Preparation of hexaalkylcyclotrisilthiane

1989-05-04

1989-12-05

Shaver, Paul F.

Organic compounds -- part of the class 532-570 series

Organic compounds

Silicon containing

C07F 708

Patent

active

048853780

ABSTRACT:
Hexaalkylcyclotrisilthiane compounds (e.g., hexamethylcyclotrisilthiane) are synthesized by reaction of lithium disulfide and a dihalodialkylsilane (e.g., dichlorodimethylsilane) in a non-oxygenated solvent (e.g., acetonitrile).

REFERENCES:
patent: 2567724 (1951-09-01), Moody
patent: 3344161 (1967-09-01), Moedritzer et al.
patent: 3506699 (1970-04-01), Viventi
Wieber et al., "Berichte", 96, 1963, pp. 1019-1021.
Giolando et al., "Inorg. Chem.", 26, No. 19, 1987, pp. 3080-3082.

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