Organic compounds -- part of the class 532-570 series – Organic compounds – Halogen containing
Patent
1988-11-28
1990-06-26
Evans, J. E.
Organic compounds -- part of the class 532-570 series
Organic compounds
Halogen containing
570127, C07C 1720, C07C 2502
Patent
active
049373978
ABSTRACT:
Chlorofluorobenzenes and difluorobenzenes are prepared by contacting a dichlorobenzene with an effective amount of KF or CsF in a polar aprotic solvent at an elevated temperature under substantially anhydrous conditions. The product can be removed as it is formed or the reaction may be run at the autogenous pressures generated by the reaction mixture in a sealed reactor.
REFERENCES:
patent: 3574775 (1971-04-01), Fuller
patent: 4369145 (1983-01-01), Souls
patent: 4590315 (1986-05-01), Moul et al.
Shiley et al. "J. Fluorine Chem.", pp. 2,19 (1972/73).
Starr et al. "Chemistry & Industry", 1328, Jul. 21, 1962.
Gall James A.
Pews R. Garth
Brookens Ronald G.
Evans J. E.
Mixan Craig E.
The Dow Chemical Company
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