Preparation of copper 2-alkoxyisobutylisonitrile complexes and .

Details Preparation of copper 2-alkoxyisobutylisonitrile complexes and . Preparation of copper 2-alkoxyisobutylisonitrile complexes and .

1993-01-13

1994-09-13

Geist, Gary

Organic compounds -- part of the class 532-570 series

Organic compounds

Radioactive metal containing

C07F 1300

Patent

active

053469950

ABSTRACT:
A new method for synthesizing 2-alkoxyisobutylisonitrile is provided in which isobutylene is used as the starting material. The haloalkoxylation of isobutylene in alcohol medium gives 2-alkoxyisobutylhalide which is then converted to 2-alkoxyisobutylamine. In the basic condition, the reaction of 2-alkoxyisobutylamine with chloroform produces 2-alkoxyisobutylisonitrile. The synthesis process contains three steps by which a higher yield is achieved. 2-Alkoxyisobutylisonitrile is labelled with technetium-99m by exchange labelling of stable tetrakis(2-alkoxyisobutylisonitrile)copper(I) complex. Tetrakis(2-alkoxyisobutylisonitrile)copper(I) complex can be prepared by the exchange of acetonitrile molecules in tetrakis(acetonitrile)copper(I) complex with isonitrile ligands.

REFERENCES:
Van Wyk et al, International Journal of Applied Radiation and Isotopes, vol. 42 (1991), pp. 687-689.

Affiliated with

Also associated with

Rating

Preparation of copper 2-alkoxyisobutylisonitrile complexes and . does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Preparation of copper 2-alkoxyisobutylisonitrile complexes and ., we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Preparation of copper 2-alkoxyisobutylisonitrile complexes and . will most certainly appreciate the feedback.

Rate now

Comments { 0 }

Profile ID: LFUS-PAI-O-1121323