Preparation of concentrated, stable water-in-oil emulsions of wa

Distillation: processes – separatory – Distilling to separate or remove only water – From organic compound

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203 52, 203 68, 203 69, 203 70, 203 91, 523332, 524801, 524827, 524831, C07B 500

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active

046455680

ABSTRACT:
Concentrated, stable water-in-oil emulsions of water-soluble or water-swellable polymers are prepared by polymerization of one or more water-soluble ethylenically unsaturated monomers in a water-in-oil emulsion and removal of water from the water-in-oil polymer emulsion by azeotropic distillation, by a method in which superheated vapor of an inert organic solvent which is immiscible with water is passed into the water-in-oil polymer emulsion. Using the process, it is also possible to concentrate emulsions which tend to coagulate or water-in-oil emulsions which are sensitive to shearing, without the polymers losing their effectiveness.

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patent: 4176107 (1979-11-01), Buckman et al.
patent: 4376850 (1983-03-01), Sanner
patent: 4435528 (1984-03-01), Domina

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