Preparation of catalyst and use for high yield conversion of...

Details Preparation of catalyst and use for high yield conversion of... Preparation of catalyst and use for high yield conversion of...

2007-07-31

2007-07-31

Parsa, J. (Department: 1621)

Chemistry of hydrocarbon compounds

Unsaturated compound synthesis

C585S530000, C585S700000

Reexamination Certificate

active

11594678

ABSTRACT:
A perovskite catalyst is prepared using a ceramic sol-sol methodology comprising preparing slurry in water of an alkaline earth metal salt, a powdered metal salt and a powdered transition metal oxide, adding a polymeric binder to form a paste, drying and comminuting the paste into a powder and heating the powder with a temperature profile to calcination temperatures. In one embodiment the slurry is formed of titanium oxide with barium carbonate and tin chloride in deionized water, and more specifically by a mixture according to Ba (1-0.05x)+TiO2+SnCl2(0.05x) where x is in moles. The perovskite catalyst is preferably used in a process for oxidative coupling of methane. Catalyst performance is enhanced through the addition of halides to the feed gas in the reaction.

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