Preparation of benzothiazolylazoanilines

Organic compounds -- part of the class 532-570 series – Organic compounds – Azo

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534581, 534582, C09B 4100

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055979050

ABSTRACT:
Described is a process for preparing benzothiazolylazoanilines by diazotization of 2-aminobenzothiazoles in a mixture consisting essentially of phosphoric acid, sulfuric acid and water using customary diazotizing agents and subsequent addition of the reaction mixture to an aqueous acidic solution of the anilines.

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Arnold T. Peters et al., "Disperse Dyes: 4-Hetarylazo Derivatives from N-.beta.-Cyanoethyl-N-.beta.-Hydroxyethylaniline", J. Chem. Tech. Biotechnol., vol. 53, pp. 301-308, 1992.
Jolanta Sokolowska-Gajda et al., "A New Medium for the Diazotization of 2-Amino-6-Nitrobenzothiazole and 2-Aminobenzothiazole", Dyes and Pigments, vol. 20, pp. 137-145, 1992.

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