Preparation of aqueous hydroxylamine solutions

Chemistry: electrical and wave energy – Processes and products – Electrostatic field or electrical discharge

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204101, 204102, 2041825, B01D 1302

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active

046455795

ABSTRACT:
Aqueous solutions of hydroxylamine are prepared from aqueous hydroxylammonium salt solutions by electrodialysis by a method in which the aqueous hydroxylammonium salt solution is fed into the middle zone of an electrolysis cell, which is divided into a cathode zone, an anode zone and a middle zone by means of semipermeable membranes, and is electrolyzed, and the catholyte used is an alkali metal hydroxide solution containing ammonia and/or amines.

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patent: 3766038 (1973-10-01), Beck et al.
patent: 4521285 (1985-06-01), De Witt et al.
Chemical Abstracts, vol. 102, 1985, abstract No. 134403s, Stamicarbon, B. V., "Circulating Process for Preparing and Working Up a Hydroxylammonium Salt Solution".
Chemical Abstracts, vol. 94, 1981, abstract No. 141,981y, Chang, Y. et al, "Conversion of Hydroxylamine Hydrochloride to Hydroxylamine Nitrate by Electrodialysis and Water Splitting".
Chemical Abstracts, vol. 83, 1975, abstract No. 181595e, Maurel, A., "Continuous Transformation of a Hydroxylamine Salt into Another Hydroxylamine Salt".
Y. Chang et al., "Chemical Abstracts", Band 94, (1981), p. 134.

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