Preparation of amine alanes

Details Preparation of amine alanes Preparation of amine alanes

1990-09-28

1992-08-04

Lee, Mary C.

Organic compounds -- part of the class 532-570 series

Organic compounds

Heterocyclic carbon compounds containing a hetero ring...

556170, 556171, 556176, C07D20700, C07F 506

Patent

active

051360462

ABSTRACT:
Tertiary amine alanes are produced by reacting sodium aluminum hydride and magnesium dichloride. A tertiary amine is admixed to extract the tertiary amine alane. Stoichiometric ratios of sodium aluminum hydride to magnesium dichloride can be varied to effect the magnesium compound by-product produced.

REFERENCES:
patent: 3355262 (1967-11-01), Beaird et al.
Everett M. Marlett and Won Suh Park, "Dimethylethylamine-Alane and N-Methyl-pyrrolidien-Alane. A Convenient Synthesis of Alane, a Useful Selective Reducing Agent in Organic Synthesis." The Journal of Organic Chemistry, 1990, vol. 55.

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