Preparation of alkyl perbromates

Details Preparation of alkyl perbromates Preparation of alkyl perbromates

1976-01-21

1977-05-10

Phillips, Delbert R.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

423476, C07C 7100

Patent

active

040228118

ABSTRACT:
Derivatives of perbromic acid of the formula: XBrO.sub.4 wherein X is Ag, H.sub.3).sub.2 CH, or (CH.sub.3).sub.2 C.sub.2 H.sub.3 prepared by a synthesis of silver perbromate through the reaction of dilute aqueous perbromic acid with silver oxide at a temperature from 0.degree. to 50.degree. C, followed by a removal of water and by a synthesis of isopropyl or isobutyl perbromate through the reaction of anhydrous silver perbromate suspended in a fluid selected from the class consisting of carbon tetrachloride, cyclohexane, and 1,1,2-trichlorotrifluoroethane with an alkyl bromide at a temperature from -25.degree. to 0.degree. C. Isopropyl and isobutyl perbromates are useful as oxidizing agents for alcohols.

REFERENCES:
baum et al., J. A. Chem. Soc., vol. 96, (1974), pp. 3233-3236.

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