Preparation of alkali metal and alkaline earth metal salts of ac

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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560 20, 560 61, 560113, 560142, C07C14390, C07C 7946, C07C 6976

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045885311

ABSTRACT:
Alkali metal and alkaline earth metal salts of acyloxybenzenesulfonic acids of the formula I ##STR1## where R is a saturated or unsaturated alkyl radical of 1 to 17 carbon atoms or is phenyl which is unsubstituted or monosubstituted or disubstituted by alkyl of 1 to 3 carbon atoms, halogen, methoxy or nitro, are prepared by neutralization, by a method in which a liquid acyloxybenzenesulfonic acid of the formula I and an aqueous solution of an alkali metal or alkaline earth metal hydroxide, carbonate or bicarbonate are combined in water, at from 0.degree. to 60.degree. C. and while mixing throughly, so that the pH is kept at from 2.5 to 7.0, and, if desired, the resulting salt is isolated from the aqueous solution in a conventional manner.

REFERENCES:
patent: 2716126 (1955-08-01), De Groote
patent: 3394155 (1968-07-01), Cahn et al.
patent: 3503888 (1970-03-01), Miller et al.
patent: 3636016 (1972-01-01), McGuire
patent: 3775445 (1973-11-01), McGuire et al.
patent: 4321157 (1982-03-01), Harris et al.

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