Preparation of aliphatic perchlorates and of trifluoromethane su

Details Preparation of aliphatic perchlorates and of trifluoromethane su Preparation of aliphatic perchlorates and of trifluoromethane su

1976-01-08

1979-08-21

Thomas, Jr., James O.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260456F, C07C 7100

Patent

active

041653327

ABSTRACT:
The formation of predominantly primary aliphatic perchlorates and trifluoethanesulfonates by reacting the corresponding silver salt with primary aliphatic halides in benzene at a temperature from about 5.degree. C. to about 50.degree. C. Primary aliphatic perchlorates and trifluoromethanesulfonates are excellent alkylating agents for amines, alcohols, and nitroalcohols.

REFERENCES:
patent: 2732398 (1956-01-01), Brice et al.
Beard et al, J. Org. Chem., vol. 39, No. 26, Dec. 27, 1974.
Burdon et al, Tetrahedron, vol. 21, pp. 1-4, Pergamon Press, Ltd., (1965).
Dafforn et al., Tetra. Letter, (36), 3159-3162, (1970).
Gramstad et al, J. Chem. Soc., 173 (1956).

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