Preparation of alcoholic hydroxylamine solution from hydroxylamm

Details Preparation of alcoholic hydroxylamine solution from hydroxylamm Preparation of alcoholic hydroxylamine solution from hydroxylamm

1985-09-09

1987-11-17

Doll, John

Compositions

Compositions containing a single chemical reactant or plural...

Organic reactant

423387, 423545, 423551, 564259, C01B 2114

Patent

active

047072946

ABSTRACT:
Solid hydroxylammonium sulfate is reacted with an alcohol solution of an alkali metal hydroxide or alkoxide to produce an alcoholic hydroxylamine liquid phase and a sulfate-containing solid phase. The liquid phase may be used for further reactions such as oxidations, hydroxamic acid production or neutralization to other hydroxylammonium salts. The different bases behave differently with regard to suitable and preferable solvents and temperatures.

REFERENCES:
patent: 4551323 (1985-11-01), Mathew et al.

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