Preparation of alcoholic hydroxylamine solution from hydroxylamm

Details Preparation of alcoholic hydroxylamine solution from hydroxylamm Preparation of alcoholic hydroxylamine solution from hydroxylamm

1982-11-01

1985-11-05

Doll, John

Chemistry of inorganic compounds

Nitrogen or compound thereof

Oxygen containing

423545, 423551, C01B 2114

Patent

active

045513236

ABSTRACT:
Solid hydroxylammonium sulfate is reacted with an alcohol solution of an alkali metal hydroxide or alkoxide to produce an alcoholic hydroxylamine liquid phase and a sulfate-containing solid phase. The liquid phase may be used for further reactions such as oxidations, hydroxamic acid production or neutralization to other hydroxylammonium salts. The different bases behave differently with regard to suitable and preferable solvents and temperatures.

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patent: 4507248 (1985-03-01), Mathew et al.
Feiser, Introduction to Organic Chemistry (1957), D. C. Heath and Co., pp. 96, 97.
Kirk-Othmer, Encyclopedia of Chemical Technology, Second Edition. vol. 11 (1967), Interscience Publishers, pp. 494-496.

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