Preparation of 2-exo-Hydroxy-7-oxabicyclo[2.2.1]heptanes

Details Preparation of 2-exo-Hydroxy-7-oxabicyclo[2.2.1]heptanes Preparation of 2-exo-Hydroxy-7-oxabicyclo[2.2.1]heptanes

1983-12-08

1984-12-11

Raymond, Richard L.

Organic compounds -- part of the class 532-570 series

Organic compounds

Heterocyclic carbon compounds containing a hetero ring...

C07D49308

Patent

active

044879458

ABSTRACT:
2-exo-Hydroxy-7-oxabicyclo[2.2.1]heptanes are prepared by treating the corresponding cis-epoxycyclohexanol with acid in an inert solvent or by treating a 3-cyclohexen-1-ol which will produce the corresponding cis-epoxy alcohol successively or concurrently with an oxidizing agent and an acid in an inert solvent.

REFERENCES:
patent: 4170599 (1979-10-01), Bennett
Wilson III, Charles W. et al., Aust. J. Chem., 28, pp. 2539-2542 (1975).
MacRae, Ian C. et al., Aust. J. Chem., 32, pp. 917-922 (1979).
Garside, J. Chem. Soc. (c), 1969, pp. 716-721.

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