Preparation of 2,4,6-trinitro-2,4,6-triaza-cyclohexanone

Details Preparation of 2,4,6-trinitro-2,4,6-triaza-cyclohexanone Preparation of 2,4,6-trinitro-2,4,6-triaza-cyclohexanone

1990-01-29

1995-02-21

Tucker, Philip

Organic compounds -- part of the class 532-570 series

Organic compounds

Four or more ring nitrogens in the bicyclo ring system

C07D25108

Patent

active

053917367

ABSTRACT:
A method for the preparation of 2,4,6-trinitro-2,4,6-triaza-cyclohexanone yielding a product with a low concentration of impurities which results in improved thermal stability is disclosed, the method involving the use of either 2-nitroimino-5-nitrohexahydro-1,3,5-triazine or an acid salt of 2-nitroimino-hexahydro-1,3,5-triazine as starting materials, with a mixture of reagents comprising (CF.sub.3 CO).sub.2 O and either HNO.sub.3 or NH.sub.4 NO.sub.3. The product is advantageous compared with RDX and HMX since it is more energetic and has a higher density.

REFERENCES:
patent: 2016521 (1935-10-01), Steindorff et al.
patent: 3696101 (1972-10-01), Litt et al.
patent: 3899489 (1975-08-01), Horlein et al.
patent: 4084054 (1978-04-01), Frump

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