Preparation of 2,3-dihydro-2,2-dimethyl-7-benzofuranyl chlorofor

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

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C07D30786

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053328418

ABSTRACT:
A process for the production of 2,3-dihydro-2,2-dimethyl-7-benzofuranyl chloroformate which comprises treating 2,3-dihydro-2,2-dimethyl-7-benzofuranol and phosgene in a water immiscible organic medium with aqueous base and removing aqueous phase from the organic phase during the process.

REFERENCES:
patent: 5066819 (1991-11-01), Kulkarni et al.
Chemical Abstract 57:11106d (1962); Ger. 1,117,598, Nov. 23, 1961.
Chemical Abstracts 59:4139f (1963); Belg. 625,406, Mar. 14, 1963.
Chemical Abstracts 59:11673c (1963); Yuki Gosei Kagaku Kyokai Shi 21(8) 611-16 (1963).
Reasenberg and Goldberg, "Esters of .beta.-Alkyaminoethanols", Journal of the American Chemical Society, 67, 933-9 (1945).

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