Preparation of 2,2'-dithiobis(benzothiazole) in an acidic aqueou

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

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C07D41712

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active

047556080

ABSTRACT:
There is disclosed a preparation of (optionally substituted) 2,2'-dithiobis(benzothiazole) by the oxidation of 2-mercaptobenzothiazole using bromate salts as the oxidant in an acidified aqueous reaction medium. The process of this invention provides an efficient and practical step in a procedure for the production of 2,2'-dithiobis(benzothiazole) that is virtually pollution free.

REFERENCES:
patent: 2064395 (1936-12-01), Tschunkur et al.
patent: 2633447 (1953-03-01), Head
patent: 4042319 (1977-08-01), Baum et al.
patent: 4337344 (1982-06-01), Alicot et al.

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