Preparation of 1,4-butanediol mono(meth)acrylate by esterificati

Details Preparation of 1,4-butanediol mono(meth)acrylate by esterificati Preparation of 1,4-butanediol mono(meth)acrylate by esterificati

1995-10-10

1997-06-10

Killos, Paul J.

Organic compounds -- part of the class 532-570 series

Organic compounds

Carboxylic acid esters

C07C 6748

Patent

active

056377606

ABSTRACT:
1,4-butanediol mono(meth)acrylate is prepared by esterification of (meth)acrylic acid with 1,4-butanediol, by a process in which an aqueous solution of unconverted 1,4-butanediol is obtained, wherein the 1,4-butanediol present in the aqueous solution is converted into readily volatile tetrahydrofuran in the presence of a catalytic amount of a strong acid and the tetrahydrofuran is separated off from the aqueous solution.

REFERENCES:
Lehrbuch der organischen Chemie, C.R. Noller, Springer Verlag, Heidelberg, 1960, pp. 639-692.

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