Chemistry: electrical and wave energy – Processes and products – Processes of treating materials by wave energy
Patent
1980-07-10
1981-08-18
Williams, Howard S.
Chemistry: electrical and wave energy
Processes and products
Processes of treating materials by wave energy
564414, 564457, B01J 1912
Patent
active
042844843
ABSTRACT:
1,3,5,7--Tetraacetamidoadamantane is prepared by reacting 1,3,5,7--tetraiadamantanewith acetonitrile and water in the presence of actinic radiation. The 1,3,5,7--tetraacetamidoadamantane can be hydrolyzed with hydrochloric acid to produce 1,3,5,7--tetraaminoadamantane tetrahydrochloride, which can be converted to the free base by treatment with an equivalent amount of an alkali, e.g. aqueous sodium hydroxide.
REFERENCES:
patent: 3419611 (1968-12-01), Moore
patent: 3523137 (1970-08-01), Moore
patent: 3591642 (1971-07-01), Szinai et al.
patent: 3985803 (1976-10-01), Inamoto et al.
Stetter et al., Chem. Ber. 93 (1960), p. 1366.
Edelberg Nathan
Erkkila A. Victor
Gibson Robert P.
The United States of America as represented by the Secretary of
Williams Howard S.
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