Preparation and isolation of mineral acid salt of an amino acid

Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acid esters

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560155, 560169, 560170, 560171, C07C10332, C07C10102, C07C10126, C07C10130

Patent

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051130092

ABSTRACT:
A cyclical process for producing and isolating a mineral acid salt of an amino acid methyl ester in high purity and yield from the reaction solution produced by esterifying an amino acid with methanol in methanol in the presence of a mineral acid, by cooling the resulting reaction solution to precipitate crystals of the mineral acid salt; filtering the crystals;

REFERENCES:
patent: 2561323 (1951-07-01), Waller et al.
patent: 2738363 (1956-03-01), Gudefroi
patent: 4154956 (1979-05-01), Veda et al.
Nippon Kagaku Zasshi (Nikkashi) 83 1151-4 (1962), Jun. 29, 1989, Chemical Abstracts Abstract.

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