Powder mixture for use in compaction to produce rare earth iron

Specialized metallurgical processes – compositions for use therei – Compositions – Loose particulate mixture containing metal particles

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252 6255, 428403, B22F 100

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054862248

ABSTRACT:
To a fine R--Fe--B alloy powder comprised predominantly of 10-30 atomic % of R (wherein R stands for at least one element selected from rare earth elements including yttrium), 2-28 atomic % of B, and 65-82 atomic % of Fe in which up to 50 atomic % of Fe may be replaced by Co, at least one boric acid ester compound such as tributyl borate is added as a lubricant in a proportion of 0.01%-2% by weight and mixed uniformly before, during, or after fine grinding of the alloy powder. The resulting powder mixture is compacted by compression molding in a magnetic field and the green compacts are sintered and aged. Compression molding can be performed continuously without need of mold lubrication, and the resulting magnets have improved magnet properties with respect to residual flux density, maximum energy product, and intrinsic coercive force.

REFERENCES:
patent: 4597938 (1986-07-01), Matsuura et al.

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