Porous Si 3 N 4 producing method

Chemistry of inorganic compounds – Silicon or compound thereof – Binary compound

Reexamination Certificate

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Reexamination Certificate

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07153484

ABSTRACT:
A producing method of a porous Si3N4having high porosity and formed of Si3N4particles having a high aspect ratio includes the following steps. A compound of a rare earth element as a first sintering agent is mixed in an amount of 7.5–45 parts by mass, in terms of an oxide of the element, with respect to 100 parts by mass of Si powder to obtain mixed powder. A binder is added to the mixed powder, which is then molded into a molded body. The molded body is heated in a nitrogen atmosphere to 300–500° C. to remove the binder. The binder-removed body is heated in a nitrogen atmosphere to 1350–1500° C. for nitriding. The nitrided body is then sintered at 1750–1900° C. at a nitrogen pressure of 0.1–1 atmosphere.

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Chemical Abstract & Indexes, American Chemical Society. Columbus, US, XP000353888.
Kawai C, “Effect Of Grain Size Distribution On The Strength Of Porous SI3N4 Ceramics Composed Of Elongated Beta-SI3N4 Grains” Dec. 1, 2001, pp. 5713-5717, XP001107807.
Search Report dated May 19, 2006.

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