Polyolefin production

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Polymers from only ethylenic monomers or processes of...

Reexamination Certificate

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C526S160000, C526S161000, C526S172000, C526S351000

Reexamination Certificate

active

06894132

ABSTRACT:
Provided is a catalyst for the polymerization of olefins of general formula:in-line-formulae description="In-line Formulae" end="lead"?R″(C4R′mC5C4R′n)XMeQin-line-formulae description="In-line Formulae" end="tail"?wherein X is an hetero-atom ligand with one or two lone pair electrons selected from the elements of Group VA or VIA which can be substituted or non-substituted: (C4Rm′C5C4Rn′) is a symmetrically substituted, 3,6-substituted fluorenyl; R′ is hydrogen or hydrocarbyl radical having from 1-20 carbon atoms, a halogen, an alkoxy, an alkoxy alkyl or an alkylamino or alkylsilylo radical, each R′ may be the same or different and m and n independently are 1, 2 3 or 4, with the proviso that the bilateral symmetry is maintained; R″ is a structural bridge between X and the (C4R′mC5C4R′n) ring to impart stereorigidity; Q is a hydrocarbyl radical having 1-20 carbon atoms or is a halogen; Me is a Group IIIB, IVB, VB, or VIB metal as positioned in the Periodic Table of Elements; and Me can be in any of its theoretically possible oxidation states.Also provided are olefin monomers (particularly propylene) polymerized using these catalysts to form syndiotactic/atactic block polymers of high molecular weight and comprising at least 70% of syndiotactic triads.

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Llinas et al., Crystalline-Amorphous Block Polypropylene and Nonsymmetric arisa-Metallocene Catalyzed Polymerization, Macromolecules 1992, vol. 25, pp. 1242-1253.

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