Polymerization regulator and composition for resin

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From sulfur-containing reactant

Reexamination Certificate

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C528S378000, C528S360000

Reexamination Certificate

active

07446163

ABSTRACT:
In the present invention, an episulfide compound having, in one molecule, at least one epithio structure represented by the following Formula 2:wherein R5is C1-C10 hydrocarbylene or single bond, R6, R7and R8are each independently C1-C10 hydrocarbyl or hydrogen, Y is O, S, Se or Te, p is an integer from 1 to 5 and q is an integer from 0 to 5,is polymerized in the presence of a halide of a 13-16 group element of the long periodic table and/or a polymerization regulator represented by the following Formula 1:wherein R1, R2and R3are each C1-C10 hydrocarbyl or hydrogen, R4is C1-C10 hydrocarbylene or single bond, X is F, Cl, Br, I, As, SH, OH, C1-C10 alkoxyl, C1-C10 alkylthio, or C1-C10 mercaptoalkylthio, and m is an integer from 1 to 5, to produce a cured resin suitable as an optical material. By using the polymerization regulator, the polymerization rate of the episulfide compound can be suitably regulated to obtain a cured resin with less defect. By using the halide, the increase in the viscosity of the starting composition during the storage or the casting operation can be prevented.

REFERENCES:
patent: 5698664 (1997-12-01), Allcock et al.
patent: 6486298 (2002-11-01), Jallouli et al.
patent: 6534589 (2003-03-01), Yoshimura et al.
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patent: WO 01/70853 (2001-09-01), None
patent: WO 02/055185 (2002-07-01), None
Abstract of an article published in Wuhan Daxue Xuebeon, Ziran Kexueban.
International Search Report, dated Jul. 16, 2002, for PCT/JP/02/03388.
English Abstract of JP 2001-2784A, Jan. 9, 2001.
English Abstract of JP 2000-256463 A, Sep. 19, 2000.
English Abstract of JP 2001-163978 A, Jun. 19, 2001.
Supplementary European Search Report, for Application No. EP 02 71 3295, Dated Feb. 22, 2006.

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