Distillation: processes – separatory – Addition of material to distilland to inhibit or prevent... – For inhibiting or preventing a polymerization reaction
Patent
1981-04-06
1982-07-27
Sever, Frank
Distillation: processes, separatory
Addition of material to distilland to inhibit or prevent...
For inhibiting or preventing a polymerization reaction
203 56, 585808, 585833, 585865, 585952, B01D 334
Patent
active
043416004
ABSTRACT:
A process for distilling vinyltoluene comprising subjecting vinyltoluene to distillation conditions in the presence of a synergistic polymerization inhibiting mixture of N-nitrosodiphenylamine (NDPA) and dinitro-para-cresol (DNPC). Preferably from about 100 to about 300 ppm by weight NDPA and about 300 to about 700 ppm by weight DNPC are dissolved in the crude vinyltoluene and the resulting solution is vacuum distilled.
REFERENCES:
patent: 3988212 (1976-10-01), Watson
patent: 4182658 (1980-01-01), Watson
Cheairs M. Norwood
Cosden Technology, Inc.
Evans J. D.
Sever Frank
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