Polymer recovery from solution

Concentrating evaporators – Processes

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134 10, 134 12, 159 22, 159DIG10, 159DIG16, 202175, 202205, 202265, 203 4, 203 88, 203 91, 203 95, 528499, 528501, 528502, B01D 100

Patent

active

049098985

ABSTRACT:
A process for removing substantial quantities of volatile liquid e.g. hydrocarbon from a mixture of polymer and such liquid is provided. This process includes the initial step of introducing the mixture, and a liquid which is immiscible with the polymer, into a mixing/kneading zone provided with heated heat transfer surfaces having a temperature higher than the boiling point of the lowest boiling liquid component in the mixing/kneading zone. The mixture and the immiscible liquid are subjected to a period of continuous mixing and kneading within the mixing/kneading zone, to bring the mixture into continuously moving contact with the heat transfer surfaces. During this period of continuous mixing/kneading, the heated heat transfer surfaces are repeatedly mechanically cleaned to prevent buildup of solid polymer thereon. Volatilized liquid is vented from the mixing/kneading zone during the period of continuous mixing and kneading, and the polymer and residual liquid is subsequently discharged from the mixing/kneading zone.

REFERENCES:
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patent: 2833750 (1958-05-01), Vickers
patent: 2992679 (1961-07-01), Twaddle
patent: 3395746 (1968-08-01), Szako et al.
patent: 3457248 (1969-11-01), Kahre
patent: 3799234 (1974-03-01), Skidmore
patent: 3956060 (1976-05-01), Scoggin
patent: 4094942 (1978-06-01), Nakai et al.
patent: 4198265 (1980-04-01), Johnson
patent: 4400236 (1983-08-01), Hanamura et al.

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