Polychloroprene-polyvinyl alcohol latex

Chemistry of carbon compounds – Miscellaneous organic carbon compounds

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526202, 526224, 526295, 260 297S, 260 297H, C08L 1102

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active

041418751

ABSTRACT:
An aqueous latex, having high colloidal stability against coagulation upon addition thereto of ionic materials and having excellent adhesive characteristics for bonding metal foil to paper to form laminates, is prepared by polymerizing, in an emulsion substantially free of carboxylate soaps, (1) an aqueous suspension of chloroprene monomer optionally containing about 0.4 to 10 mole percent of alpha, beta-unsaturated carboxylic acid monomer, based on the total monomer content, (2) in the presence of (a) about 3-10 parts of polyvinyl alcohol and (b) about 0.3-2 parts of an organic, sulfur-containing chain-transfer agent of the group consisting of dialkyl xanthogen disulfides and alkyl mercaptans, both (a) and (b) being expressed in parts by weight based on 100 parts by weight of monomer (1). The polymer so produced contains 10-95% gel polymer, and the polyvinyl alcohol is present therein in a form such that it is not completely recoverable by extraction with water.

REFERENCES:
patent: 2463225 (1949-03-01), Vincent
patent: 2564291 (1951-01-01), Wolf
patent: 2902458 (1959-01-01), Teppema
patent: 3361693 (1968-01-01), Geshwind
patent: 3492276 (1970-01-01), Smith
patent: 3703568 (1972-01-01), Kadowaki et al.
patent: 3912676 (1975-10-01), Brizzolara et al.
Encyclopedia of Polymer Science and Technology, vol. 3, John Wiley & Sons, Inc., (1965), pp. 705, 708, 711.
Blackley, High Polymer Latices, (vol. I), (vol. II), pp. 113-114, 121, 122, 752, and 757 (Applied Science, 1966).

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