Pitch-only densification of carbon-carbon composite materials

Plastic and nonmetallic article shaping or treating: processes – Carbonizing to form article – With carbonizing – then adding carbonizable material and...

Reexamination Certificate

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C264S103000, C264S029100

Reexamination Certificate

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08003026

ABSTRACT:
Method for making carbon-carbon composite friction product, by: fabricating carbon fiber preform; heat-treating the carbon fiber preform; infiltrating the carbon fiber preform with a high carbon-yielding pitch using VPI (vacuum pressure infiltration) or resin transfer molding (RTM) processing; carbonizing the preform with an intermediate heat-treatment at 800-2000° C.; repeating the pitch infiltration and carbonization steps to achieve a final density of >1.75 g/cc; machining the surfaces of the preform; and applying an oxidation protection system. This approach overcomes problems inherent in lower density carbon-carbon composites by employing high carbon-yielding pitches to densify the carbon-carbon composites to a high density. The high carbon yielding pitches may include isotropic pitches, 100% anisotropic (mesophase) pitches, or mixtures of the two. They may be derived from petroleum, coal tar, or synthetic feedstocks.

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patent: 2004/0195712 (2004-10-01), La Forest et al.
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patent: 2005/0266220 (2005-12-01), La Forest et al.
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patent: 1 724 245 (2006-11-01), None
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patent: WO-2005/016476 (2005-02-01), None
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European Search Report from corresponding EP Application No. 09161254,9, mailed Oct. 8, 2009, 3 pages.
European Examination Report from corresponding EP Application No. 09161254.9, mailed Jun. 1, 2010, 7 pages.

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