Pitch-based carbon foam and composites and use thereof

Chemistry of inorganic compounds – Carbon or compound thereof – Elemental carbon

Reexamination Certificate

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Reexamination Certificate

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07070755

ABSTRACT:
A thermally conductive carbon foam is provided, normally having a thermal conductivity of at least 40 W/m·K. The carbon foam usually has a specific thermal conductivity, defined as the thermal conductivity divided by the density, of at least about 75 W·cm3/m·° K·gm. The foam also has a high specific surface area, typically at least about 6,000 m2/m3. The foam is characterized by an x-ray diffraction pattern having “doublet” 100 and 101 peaks characterized by a relative peak split factor no greater than about 0.470. The foam is graphitic and exhibits substantially isotropic thermal conductivity. The foam comprises substantially ellipsoidal pores and the mean pore diameter of such pores is preferably no greater than about 340 microns. Other materials, such as phase change materials, can be impregnated in the pores in order to impart beneficial thermal properties to the foam. Heat exchange devices and evaporatively cooled heat sinks utilizing the foams are also disclosed.

REFERENCES:
patent: 2401797 (1946-06-01), Rasmussen
patent: 3306353 (1967-02-01), Burne
patent: 3453809 (1969-07-01), Henderson
patent: 3558276 (1971-01-01), Otani et al.
patent: 3784487 (1974-01-01), Franck et al.
patent: 3914392 (1975-10-01), Klett
patent: 3973718 (1976-08-01), Deschamps
patent: 3979196 (1976-09-01), Frank et al.
patent: 4005183 (1977-01-01), Singer
patent: 4007324 (1977-02-01), Wallouch
patent: 4025689 (1977-05-01), Kobayashi et al.
patent: 4057101 (1977-11-01), Ruka et al.
patent: 4096097 (1978-06-01), Yan
patent: 4125676 (1978-11-01), Maricle et al.
patent: 4205055 (1980-05-01), Maire et al.
patent: 4225463 (1980-09-01), Unger et al.
patent: 4272356 (1981-06-01), Stiller et al.
patent: 4276246 (1981-06-01), Bonzom et al.
patent: 4303431 (1981-12-01), Torobin
patent: 4311682 (1982-01-01), Miyazaki et al.
patent: 4318824 (1982-03-01), Turner
patent: 4439349 (1984-03-01), Everett et al.
patent: 4442165 (1984-04-01), Gebhardt et al.
patent: 4487687 (1984-12-01), Simo et al.
patent: 4512388 (1985-04-01), Claar et al.
patent: 4518483 (1985-05-01), Dickakian
patent: 4525492 (1985-06-01), Rastall et al.
patent: 4550015 (1985-10-01), Korb et al.
patent: 4572864 (1986-02-01), Benson et al.
patent: 4605595 (1986-08-01), Tsang et al.
patent: RE32319 (1986-12-01), Korb et al.
patent: 4637906 (1987-01-01), Fukuda et al.
patent: 4659624 (1987-04-01), Yeager et al.
patent: 4775655 (1988-10-01), Edwards et al.
patent: 4782586 (1988-11-01), Joo et al.
patent: 4806290 (1989-02-01), Hopper et al.
patent: 4832881 (1989-05-01), Arnold, Jr. et al.
patent: 4873071 (1989-10-01), Yamada et al.
patent: 4873218 (1989-10-01), Pekala
patent: 4892783 (1990-01-01), Brazel
patent: 4917835 (1990-04-01), Lear et al.
patent: 4934657 (1990-06-01), Dodson
patent: 4978649 (1990-12-01), Surovikin et al.
patent: 4992254 (1991-02-01), Kong
patent: 4999385 (1991-03-01), McCullough, Jr. et al.
patent: 5019164 (1991-05-01), Tomita et al.
patent: 5047225 (1991-09-01), Kong
patent: 5053148 (1991-10-01), von Bonin
patent: 5071631 (1991-12-01), Takabatake
patent: 5076845 (1991-12-01), Seo et al.
patent: 5114635 (1992-05-01), Sohda et al.
patent: 5138832 (1992-08-01), Pande
patent: 5217701 (1993-06-01), Sakata et al.
patent: 5232772 (1993-08-01), Kong
patent: 5248705 (1993-09-01), McGuigan et al.
patent: 5300272 (1994-04-01), Simandl et al.
patent: 5384193 (1995-01-01), Suh et al.
patent: 5437927 (1995-08-01), Ross et al.
patent: 5487946 (1996-01-01), McGinniss et al.
patent: 5540903 (1996-07-01), Romine
patent: 5556892 (1996-09-01), Pekala
patent: 5578255 (1996-11-01), Okuyama et al.
patent: 5580500 (1996-12-01), Muramatsu et al.
patent: 5582781 (1996-12-01), Hayward
patent: 5614134 (1997-03-01), Sohda et al.
patent: 5695816 (1997-12-01), Iwashita et al.
patent: 5705106 (1998-01-01), Kolesnikov et al.
patent: 5709914 (1998-01-01), Hayes
patent: 5733484 (1998-03-01), Uchida et al.
patent: 5770127 (1998-06-01), Abrams et al.
patent: 5868974 (1999-02-01), Kearns
patent: 5882621 (1999-03-01), Doddapaneni et al.
patent: 5888430 (1999-03-01), Wakayama et al.
patent: 5888469 (1999-03-01), Stiller et al.
patent: 5902562 (1999-05-01), Lagasse et al.
patent: 5945084 (1999-08-01), Droege
patent: 5954937 (1999-09-01), Farmer
patent: 6013371 (2000-01-01), Hager et al.
patent: 6033506 (2000-03-01), Klett
patent: 6037032 (2000-03-01), Klett et al.
patent: 6077464 (2000-06-01), Murdie et al.
patent: 6126874 (2000-10-01), Dillon et al.
patent: 6142222 (2000-11-01), Kang et al.
patent: 6176268 (2001-01-01), Hsich et al.
patent: 6241957 (2001-06-01), Stiller et al.
patent: 2411811 (1979-07-01), None
patent: 408048509 (1996-02-01), None
patent: WO9827023 (1998-06-01), None
patent: WO 9911585 (1999-03-01), None
patent: WO 9911586 (1999-03-01), None
patent: WO 9964223 (1999-12-01), None
Klett, J. and Edie, D., Flexible Towpreg for the Fabrication of High Thermal Conductivity Carbon/Carbon Composities,Carbon, 33:10, pp. 1485-1503.
Hexcel Product Data Sheet (1997).
Kearns, K., Graphitic Carbon Foam Processing, 21stAnnual Conference on Composites, Materials, and Structures, Jan. 26-31, 1997, Cocoa Beach, FL, pp. 835-847 (1997).
Lake, M.L., “Simple Process Produces High Modulus Carbon Fibers at Much Lower Cost,”Mat. Tech. 11(4): 137-139 (1996).
Jones, S.P., Fain, C.C. and Edie, D.D., “Structural Development in Mosephase Pitch Based Carbon Fibers Produced from Naphthalene,” 35(10): 1533-1543 (1997).
Amoco Product Literature (1997).
Steiner, K.V. et al., “Production and Properties of Ultra-Lightweight Aluminum Foams for Industrial Applications,” Proceeding from the 4thInternational Conference on Composites Engineering, Edited by David Hul, pp. 943-944 (1997).
Inoue, K., “Application of Laser Flash Method To Penetrative Materials for Measurement of Thermal Diffusivity,”High Temp. Tech. 8(1): 21-26 (1990).
Ohihorst, C.W. et al., “Thermal Conductivity Database of Various Structural Carbon-Carbon Composite Materials,” NASA Technical Memorandum 4787 (Nov. 1997).
Mehta, R. et al., “Graphitic Carbon Foams: Processing and Characterization,” 21stBiennial Conference on Carbon, Conf. Proceedings, American Carbon Society, Buffalo, New York, pp. 104-105 (1993).
Cowan, R.D., “Pulse Method of Measuring Thermal Diffusivity at High Temperatures,” J. of App. Phys., 34(4), pp. 926-927 (1962).
Introduction to Carbon Science, ed. Harry Marsh, Butterworths and Co., Ltd., London, pp. 6-16, 39-44, 47-49, 51-52, 55-58, 61 and 109 (1989).
Brooks and Taylor, “The Formation of Graphitizing Carbons from the Liquid Phase,”Carbon, 3(2),pp. 185-193 (1965).
Rouzaud, J.N. and Oberlin, A., “Structure, Microtexture and Opitcal Properties of Anthracene and Saccharose-Based Carbons,”Carbon, 27(4), pp. 517-529 (1989).
Rand, B., “Matrix Precursors for Carbon-Carbon Composites,” inEssentials of Carbon-Carbon Composites, edited by C.R. Thomas, Royal Society of Chemistry, London pp. 67-102 (1993).
Kelly, B.T., “The Thermal Conductivity of Graphite,”Physics and Chemistry of Carbon, 5, pp. 119-215 (1969).
Adams, P.M, Katzman, H.A. and Rellick, G.S., “Microstructural and X-Ray Diffraction Studies of Carbon/Carbon Composites for Thermal Management Applications,” Aerospace Report No. ATR-98-(8565)-1, Naval Surface Warfare Center Carderock Division, Contract No. FO4701-93-C-0094, Mar. 1, 1998.
Ultramet Product Literature, 1998 (for Ultrafoam,).
Japan Patent Publication No. 04163319, published Jun. 8, 1992 (one page English abstract from European Patent Office).
Klett, J. and Edie, D., “Flexible Towpreg for the Fabrication of High Thermal Conductivity Carbon/Carbon Composities,” URL:http://www.ms.ornl.gov/cimtech/cfcms/towpreg.html. Last updated Apr. 14, 1996.
I. Mochida, Y. Korai, K. Shimizu, S. Yoon & R. Fujtura, Preparation, Structure and Application of Monophase Pitches Prepared from Aromatic Hydrocarbons Using HF/BF3 as Catalysts, Tanso, 1992, p. 370-378, No. 155.
R. Fujiura, T. Kojima,

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