Phenol purification

Distillation: processes – separatory – With disparate physical separation – Utilizing liquid-liquid extracting of distillation product

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203 46, 203 83, 203 96, 203 98, 568754, C07C 3776

Patent

active

045043647

ABSTRACT:
In the production of high purity phenol, a water-phenol mixture recovered from the top of a distillation column is contacted with a water immiscible solvent to extract methyl benzofuran and other by-products and impurities in phenol production therefrom, with the extraction being accomplished at a temperature at which the water-phenol mixture is present as a single phase liquid. The remaining mixture of phenol and water is recycled to the distillation.

REFERENCES:
patent: 2486342 (1949-10-01), Taylor et al.
patent: 3692845 (1972-09-01), Cheema et al.
patent: 3810946 (1974-05-01), Yeh et al.
patent: 4298765 (1981-11-01), Cochran et al.
patent: 4351967 (1982-09-01), Nishimura et al.

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