Parallel mass spectrometer

Radiant energy – Ionic separation or analysis

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250283, 250282, B01D 5944

Patent

active

045075557

ABSTRACT:
A parallel mass spectrometer, which consists of two or more sets of ion extraction means, mass resolution devices and ion detectors connected in parallel, is interfaced with a separation device, such as a gas chromatograph, for sample analysis. The formed sample ions are simultaneously and separately directed into first and second mass resolution devices. The first mass resolution device is operated under either total ion current or select ions monitoring mode with its detection system constantly monitoring the appearance of the chromatographic peaks. The second mass resolution device is operated under a mass scanning mode, but a mass scan operation is initiated only when a chromatographic peak occurs. Alternatively, a mass scan operation can be arranged such that only the raw mass scan data obtained in synchronization with the appearance of the chromatographic peak are acquired or processed. This allows sample qualitative and quantitative analysis to be achieved simultaneously without compromise on the performance of either the chromatograph or mass spectrometer.

REFERENCES:
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patent: 3479504 (1969-11-01), Hull
patent: 3510647 (1970-05-01), Wood
patent: 4209697 (1980-06-01), Renner et al.
patent: 4266127 (1981-05-01), Chang
patent: 4283626 (1981-08-01), Siegel
patent: 4377745 (1983-03-01), Chang
"A 15-cm Radius Mass Spectrometer Which Simultaneously Collects Positive and Negative Ions" by Harry J. Svec and Gerald D. Flesch, Journal of Mass Spectrometry and Ion Physics, 1 (1968), pp. 41-52.
"Special Techniques in the Combination of Gas Chromatography and Mass Spectrometry", by D. Henneberg, U. Henrichs and G. Schomburg, Journal of Chromatography, 112 (1975), pp. 343-352.
"Design, Implementation, and Performance of a High Resolution Gas Chromatography/High Resolution Mass Spectrometry/Real-Time Computer System for the Analysis of Complex Organic Mixtures", by J. Meili, F. C. Walls, R. McPherron and A. L. Burlingame, Journal of Chromatographic Science, 17 (1979), pp. 29-42.

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