Para-nitrobenzotribromide process

Details Para-nitrobenzotribromide process Para-nitrobenzotribromide process

1975-12-22

1976-11-23

Sebastian, Leland A.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07C 7912

Patent

active

039937046

ABSTRACT:
The conversion of p-nitrobenzal bromide to p-nitrobenzotribromide, an intermediate in the preparation of the insecticide, 1,5-bis(4-trifluoromethylphenyl)-3-cyanoformazan, by reacting p-nitrobenzal bromide with an alkali or alkaline earth metal hypobromite is improved by carrying out the reaction in a two-phase, water-organic solvent system.

REFERENCES:
patent: 3267159 (1966-08-01), Shipp

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