Alloys or metallic compositions – Palladium base
Reexamination Certificate
2008-06-03
2008-06-03
Ip, Sikyin (Department: 1793)
Alloys or metallic compositions
Palladium base
C420S464000, C420S465000, C148S430000, C148S678000
Reexamination Certificate
active
07381368
ABSTRACT:
A palladium-boron composition and methods of making and using same are provided. In one aspect, the invention comprises an alloy comprising palladium and boron, the boron being in solid solution in the palladium and the alloy having a two-phase structure, wherein each phase of the two-phase structure has the same crystal structure as the other phase and has a different set of lattice parameters from the other phase such that the palladium is greatly hardened by the presence of the smaller phase crystals within the spaces between the larger phase crystals. The composition is carefully prepared by a process wherein palladium and an amount of boron sufficient to place the boron in solid solution, but insufficient to combine with the palladium, are placed together and repeatedly are melted, cooled and turned over until sufficiently mixed. The hardened composition can be used to create thinner membranes for hydrogen purification and improved electrodes for generation of heat energy, and other electrochemical processes.
REFERENCES:
Sakamoto, Y; Baba, K.; Flanagan, Ted B., The effect of alloying of palladium on the hydrogen-palladium misibility gap, Z. Phys. Chem. (Munich) (1988), 158(2), 223-35. Cited in parent application.
Cited in parent application.
Imam M. Ashraf
Miles Melvin H.
Grunkemeyer Joseph T.
Ip Sikyin
Karasek John J.
The United States of America as represented by the Secretary of
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