Oxidaton of primary alcohols to carboxylic acids with a TEMPO ca

Details Oxidaton of primary alcohols to carboxylic acids with a TEMPO ca Oxidaton of primary alcohols to carboxylic acids with a TEMPO ca

1999-04-01

2000-10-03

Killos, Paul J.

Organic compounds -- part of the class 532-570 series

Organic compounds

Carboxylic acids and salts thereof

562409, 562416, 562422, 562490, 562526, 562491, 562493, 562556, 562561, 562609, 562621, C07C 5116

Patent

active

061275735

ABSTRACT:
The present invention relates to a TEMPO-catalyzed oxidation of primary alcohols, RCH.sub.2 OH to corresponding carboxylic acids, RCOOH in the presence of catalytic in the presence of catalytic amount of NaClO and stoichiometric amount of NaClO.sub.2 as an oxidant. ##STR1##

REFERENCES:
patent: 5631366 (1997-05-01), Lohri et al.
Wovkulich et al.; J. Org. Chem.; vol. 58; p. 832, 1993.
Nooy et al.; Synthesis; p. 1153, 1996.
Ohira, S., Synthetic Communications, vol. 19, pp. 561-564, 1989.
Muller, S., Synlett, pp. 521-522, 1996.
Anelli, P.L., et al., J. Org. Chem., vol. 52(12), pp. 2559-2562.
Dalcanale, E., et al., J. Org. Chem., vol. 51(4), pp. 567-571, 1986.
Zhao, M., et al., J. Org. Chem., vol. 64(7), pp. 2564-2566, 1999.

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