Oxidative coupling of alkylphenols catalyzed by metal complexes

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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252430, 252431N, 252431C, 260 47ET, 260613R, 568730, C07C 3700, C07C 3912, C07C 3916, C07C 4516

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041327225

ABSTRACT:
Carbon-carbon coupled self-condensation products obtained by the oxidative coupling of alkylphenols are prepared by contacting an aqueous mixture of an alkyl phenol with oxygen in the presence of sufficient alkaline material to sustain a pH in the range of 9-9.5 during the oxidative coupling reaction and a catalyst system comprising a copper, cobalt, nickel, iron, chromium, cerium or manganese complex of a diimino acid. The mixture may optionally contain a surfactant.

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