Oxidation of selectively protected 2,3-dihydro-6-methyl-8-hydrox

Details Oxidation of selectively protected 2,3-dihydro-6-methyl-8-hydrox Oxidation of selectively protected 2,3-dihydro-6-methyl-8-hydrox

1974-12-13

1976-06-08

Rush, Raymond V.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

424261, C07D45710

Patent

active

039622533

ABSTRACT:
6-Methyl-8-alkanoyloxy (or 8-hydroxy)-9-ergolenes, useful as prolactin inhibitors, are prepared from 2,3-dihydro-6-methyl-8-hydroxy-9-ergolene by selective N-acylation, selective O-acylation, selective N-deacylation, and oxidation of the selectively deacylated compound.

REFERENCES:
patent: 2864822 (1958-12-01), Fornefeld et al.
Fieser et al., Reagent for Organic Chemistry, (1967) p. 642.
Rabjohn, Organic Synthesis, vol. IV, (1963) p. 582.

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