Oxidation of N-substituted methylamines to N-substituted formami

Details Oxidation of N-substituted methylamines to N-substituted formami Oxidation of N-substituted methylamines to N-substituted formami

1975-09-22

1977-08-16

Sneed, Helen M. S.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260239B, 260268C, 26029386, 260562R, 260562P, C07C10336

Patent

active

040426211

ABSTRACT:
An N-substituted methylamine is reacted in a liquid homogeneous system with molecular oxygen in the presence of a soluble halide of certain metals to produce an N-substituted formamide. Exemplary is the reaction of trimethylamine with oxygen in the presence of cupric chloride to produce dimethylformamide.

REFERENCES:
patent: 2793211 (1957-05-01), LoCicero et al.
patent: 3483210 (1969-12-01), Rosenblatt
patent: 3530182 (1970-09-01), Haynes et al.
Rosenblatt et al., Tetrahedron Letters, vol. 38, 4085 (1968).
Yoke et al., Inorganic Chem., 2, 1210-1216 (1963).

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