Oxidation of isobutane under super-critical conditions

Details Oxidation of isobutane under super-critical conditions Oxidation of isobutane under super-critical conditions

1981-10-05

1983-09-13

Lone, Werren B.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

568565, C07C17902

Patent

active

044044062

ABSTRACT:
In the preparation of tertiary-butyl hydroperoxide by the direct oxidation of isobutane, the production of tertiary-butyl hydroperoxide, expressed as the quantity of the compound prepared per unit of reactor volume per unit of time, is enhanced by conducting the oxidation in a dense, supercritical phase reaction mixture at a temperature in excess of the critical temperature of the mixture, at a pressure in excess of the critical pressure of the mixture, and under conditions relating to composition of the mixture.

REFERENCES:
patent: 2845461 (1958-07-01), Winkler et al.
patent: 3478108 (1969-11-01), Grane
patent: 3502740 (1970-03-01), Zajacek et al.
patent: 3816540 (1974-06-01), Barone
patent: 3855314 (1974-12-01), Dubois
patent: 3907902 (1975-09-01), Grane
patent: 3974228 (1976-08-01), Barone
patent: 4128587 (1978-05-01), Jubin
Winkler, "Industrial and Eng. Chem.", vol. 53, (1961), p. 655.

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