Oxidation of allylacetone to 2,5-hexanedione in a water-carbon t

Details Oxidation of allylacetone to 2,5-hexanedione in a water-carbon t Oxidation of allylacetone to 2,5-hexanedione in a water-carbon t

1974-04-08

1976-08-03

Thomas, Jr., James O.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260597R, C07C 4500, C07C 4504

Patent

active

039729427

ABSTRACT:
An economical process is described for the oxidation of allylacetone to 2,5-hexanedione in a solvent system which is a mixture of water and carbon tetrachloride and employing palladium chloride as the oxidation catalyst. High yields of product are obtained with minimal losses of the expensive palladium catalyst.

REFERENCES:
patent: 3301905 (1967-01-01), Reimenschneider et al.
patent: 3303020 (1967-02-01), Clement et al.
patent: 3701810 (1972-10-01), Hasegawa et al.
Yamamoto et al., Kogyo Kakaku Yasshi, vol. (71(6), pp. 945-946, (1968).
Smidt et al., Angewante Chem., vol. 71(5), pp. 176-182, (1959).

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