Oxidation and sinter-resistant metal powders and pastes

Specialized metallurgical processes – compositions for use therei – Processes – Electrothermic processes

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252472, B22F 900, B01J 2374

Patent

active

040100251

ABSTRACT:
A high density precious metal powder that resists sintering at 600.degree. C. and contains a very small percentage of titania or zirconia is produced by co-nucleation and precipitation of gold and titania from an ammoniacal solution at pH 3-4 with a bisulfite.
A nickel powder including a very small percentage of a refractory oxide such as zirconia is prepared by co-nucleation and precipitation from an alkaline solution with hydrazine.
Materials so prepared have oxidation resistance and sintering temperatures superior to the pure metal, and find utility in microelectronics as air-fired thick films. Nickel powders so prepared are also useful as hydrogenation catalysts and in other applications.

REFERENCES:
patent: 2564331 (1951-08-01), Hawley
patent: 3235515 (1966-02-01), Taylor

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